Abstract: respectively oxide, carbon and metal oxides, carbon materials, to study the feasibility of carbon oxides Al2OC microwave heating as a means of synthesis, the effect is composed of two different materials, optimizing the synthesis conditions. Sintered product was analyzed by XRD phase, morphology was observed by SEM and EDX analysis for determining elemental composition point. The results show that: when the oxide, carbon materials under 1700 ℃ can generate carbon oxides Al4C3 but not observed when metal oxides, carbon materials can be observed under 1500 ℃ and carbon oxides Al4C3 Al2OC.(carbide powder)

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